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[CAS Name] Gliclazide

[Formula] C15H21N3O3S

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[CAS Name]Gliclazide
[Alias]1-(3-Azabicyclo[3.3.0]oct-3-yl)-3-(p-tolylsulfonyl)urea; 1-(Hexahydrocyclopenta[c]pyrrol-2(1H)-yl)-3-(p-tolylsulfonyl)urea; Benzenesulfonamide, N-(((hexahydrocyclopenta(c)pyrrol-2(1H)-yl)amino)carbonyl)-4-methyl-; benzenesulfonamide, N-[[(hexahydrocyclopenta[c]pyrrol-2(1H)-yl)amino]carbonyl]-4-methyl-; N-(4-Methylbenzenesulfonyl)-N'-(3-azabicyclo[3.3.0]oct-3-yl)urea; N-[(hexahydrocyclopenta[c]pyrrol-2(1H)-ylamino)carbonyl]-4-methylbenzenesulfonamide; N-[[(Hexahydrocyclopenta[c]pyrrol-2(1H)-yl)amino]carbonyl]-4-methylbenzenesulfonamide; N-(hexahydrocyclopenta[c]pyrrol-2(1H)-ylcarbamoyl)-4-methylbenzenesulfonamide
[Number]21187-98-4
[EINECS]244-260-5
[Formula]C15H21N3O3S
[Molecular weight]323.4105

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Shandong Ruiying Pharmaceutical Group Co., Ltd.

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Chuming Pharmaceutical Limited

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Shanghai Agrotree Chemical Co., Ltd

ITEMS	RESULTS
Characteristics	A white powder
Solubility	Practically insoluble in water: freely soluble in methylene chloride; Sparingly soluble in acetone(96%); slightly soluble in alcohol (96%)
M.P	164.0-164.5°C
Identification	Conform to the spectrum of the CRS Gliclazide
Heavy metals	<10ppm
Impurity B	0.3ppm
Related substances	<0.10%
	<0.10%
	0.13%
Loss on drying	0.1%
Sulphated ash	0.01%
Residual solvents	Below LOQ
Residual solvents	Below LOQ
Assay (on dried basis)	99.5%
Conclusion	The test results conform with EP/BP/CP